锻压技术

一种奥氏体-马氏体(A-M)型双相不锈钢专用冷拔细丝润滑剂的研发

英文标题：Development on special lubricant of fine wire cold-drawing for

分类号：TH117.22

出版年,卷(期):页码：2018,43(11):120-126

摘要：

为了改善奥氏体-马氏体(A-M)型双相不锈钢冷拔细丝工艺中的润滑性能，减少冷拔机和器件的磨损，提高奥氏体-马氏体(A-M)型双相不锈钢表面的光洁度，研制了一种奥氏体-马氏体(A-M)型双相不锈钢冷拔细丝工艺专用润滑剂。通过采用L-AN22#全损耗系统用油作为基础油，并选择了合适的极压剂、抗磨剂、抗氧剂及摩擦改进剂等功能添加剂，经调和后得到研制润滑剂。经各项理化性能测试和冷拔模拟试验可知，研制润滑剂能满足奥氏体-马氏体(A-M)型双相不锈钢在冷拔细丝过程中对加工质量的的要求。冷拔后细丝表面光泽度较高，研制油在油膜承载能力、退火清净性等各方面优于参比油，可达到预期效果。

In order to improve the lubrication performance of austenitic-martensitic (A-M) duplex stainless steel, reduce the wear of cold-drawing machine and dies in the cold-drawing process of fine wire and improve the surface roughness of fine wire, a special lubricant was developed. Then, taking the L-AN22# lubricating oils for total loss system as the base oil, the developed lubricant was prepared by blending with appropriate functional additives such as extreme pressure agent, anti-wear agent, antioxidant and friction modifier. The physical and chemical properties and cold-drawing simulation tests show that the developed lubricant meets the quality requirement in the cold-drawing process of fine wire for the austenitic-martensitic duplex stainless steel well. After cold-drawing, the surface roughness of the fine wire is relatively high, and the developed oil is superior to the reference oil in terms of oil film carrying capacity and annealing detergency, which achieves the desired results.

基金项目：

广西石化资源加工及过程强化技术重点实验室开放基金（2017K009）；广西科技计划项目技术创新引导专项（2017AC05020）

胡雄风（1992-），男，硕士研究生,E-mail：huxiongfeng1992@163.com;通讯作者：黄福川（1963-），男，博士，教授,E-mail：huangfuchuan@gxu.edu.cn

参考文献：

［1］严彪. 不锈钢手册(精)
［M］. 北京:化学工业出版社, 2009.

Yan B. Stainless Steel Handbook
［M］. Beijing:Chemical Industry Press, 2009.

［2］Wang S, Ge Z, Ren X, et al. Analysis of magnetic particle indication about 15-5PH precipitation-hardening stainless steel
［J］. Journal of Aeronautical Materials, 2015, 35(1)：77-81.

［3］徐效谦, 阴绍芬. 特殊钢钢丝
［M］. 北京:冶金工业出版社, 2005.

Xu X Q, Yin S F. Special Steel Wire
［M］. Beijing:Metallurgical Industry Press, 2005.

［4］Kalpakjian S, Vijai Sekar K S, Schmid S R. Manufacturing Engineering and Technology
［M］. New Jersey:Pearson, 2014.

［5］杨德崇. 不锈钢丝拉拔润滑剂
［J］. 合成润滑材料, 2007, 34(1): 33-36.

Yang D C. Drawing lubricants for stainless steel wire
［J］. Synthetic Lubricants, 2007, 34(1): 33-36.

［6］Shokoohi Y, Khosrojerdi E, Shiadhi B H R. Machining and ecological effects of a new developed cutting fluid in combination with different cooling techniques on turning operation
［J］. Journal of Cleaner Production, 2015, 94: 330-339.

［7］Tan C J, Abe Y, Daodon W, et al. Increase in ironing limit of aluminium alloy cups with lubricants containing nanoparticles
［J］. Journal of Materials Processing Technology, 2016, 229: 804-813.

［8］Srikant R R, Rao P N. Use of Vegetable-Based Cutting Fluids for Sustainable Machining
［M］. Berlin: Springer International Publishing, 2017.

［9］Guan J, Xu X, Hu J, et al. Preparation and action mechanism of inclusion complex of β-cyclodextrin and sulfurized isobutylene as additives in solution of polyethylene glycol-600
［J］. Journal of Wuhan University of Technology-Mater. Sci. Ed., 2015, 30(4):859-867.

［10］NB/SH/T 0189—2017, 润滑油抗磨损性能的测定四球法
［S］.

NB/SH/T 0189—2017, Standard test method for wear preventive characteristics of lubricating fluid—Four-ball method
［S］.

［11］GB/T 12583—1998, 润滑剂极压性能测定法(四球法)
［S］.

GB/T 12583—1998, Standard test method for measurement of extreme-pressure properties of lubricating fluid (four-ball method)
［S］.

［12］晁绵冉, 苏怀刚, 李维民, 等. 3种烷基二苯胺类抗氧剂的合成与性能
［J］. 精细化工, 2013, 30(1): 108-112.

Yao M R, Shu H G, Li W M,et al. Synthesis and properties of three kinds of alkyl diphenylamine as antioxidant
［J］. Fine Chemicals, 2013, 30(1): 108-112.

［13］SH/T 0193—2008, 润滑油氧化安定性的测定旋转氧弹法
［S］.

SH/T 0193—2008, Lubricating oils-Determination of oxidation stability-Rotating pressure vessel method
［ S］.

［14］Spikes H. Friction modifier additives
［J］. Tribology Letters, 2015, 60(1): 5.

［15］GB/T 265—1988, 石油产品运动粘度测定法和动力粘度计算法
［S］.

GB/T 265—1988, Petroleum products-Determination of kinematic viscosity and calculation of dynamic viscosity
［S］.

［16］GB/T 1995—1998, 石油产品粘度指数计算法
［S］.

GB/T 1995—1998, Petroleum products-Calculation of viscosity index
［S］.

［17］GB/T 3536—2008, 石油产品闪点和燃点的测定克利夫兰开口杯法
［S］.

GB/T 3536—2008, Petroleum products—Determination of flash and fire points—Cleveland open cup method
［S］.

［18］GB/T 3535—2006, 石油产品倾点测定法
［S］.

GB/T 3535—2006, Petroleum products-Determination of pour point
［S］.

［19］GB/T 7325—1987, 润滑脂和润滑油蒸发损失测定法
［S］.

GB/T 7325—1987, Petroleum products-Lubricating greases and oils-Determination of evaporation loss
［S］.

［20］GB/T 511—2010, 石油和石油产品及添加剂机械杂质测定法
［S］.

GB/T 511—2010, Petroleum products and additives-Method for determination of mechanical admixtures
［S］.

［21］GB/T 260—2016, 石油产品水含量的测定蒸馏法
［S］.

GB/T 260—2016, Test method for water in petroleum products-Distillation method
［S］.

［22］GB/T 5096—2017, 石油产品铜片腐蚀试验法
［S］.

GB/T 5096—2017, Petroleum products—Corrosiveness to copper-Copper strip test
［S］.

［23］GB/T 7304—2014, 石油产品酸值的测定电位滴定法
［S］.

GB/T 7304—2014, Standard test method for acid number of petroleum products potentiometric titration
［S］.

［24］GB/T 3142—1982, 润滑剂承载能力测定法 (四球法)
［S］.

GB/T 3142—1982, Lubricants—Determination of load-carrying capacity (four balls method)
［S］.

［25］SH/T 0762—2005, 润滑油摩擦系数测定法(四球法)
［S］.

SH/T 0762—2005, The test method of determination of the coefficient of friction of lubricants using the four-ball wear test machine
［S］.

［26］GB/T 17144—2004, 石油产品残炭测定法(微量法)
［S］.

GB/T 17144—2004, Petroleum products—Determination of carbon residue-Micro method
［S］.

［27］GB/T 11143—2008, 加抑制剂矿物油在水存在下防锈性能试验法
［S］.

GB/T 11143—2008, Standard test method for rust-preventing characteristics of inhibited mineral oil in the presence of water
［S］.

［28］NB/SH/T 0306—2013，润滑油承载能力的评定FZG目测法
［S］.

NB/SH/T 0306—2013，Standdard test method for evaluating the scctffing load capacity of oils (FZG visaal method)
［S］

［29］GB/T 12579—2002，润滑油泡沫特性测定法
［S］.

GB/T 12579—2002，Determination of foaming characterisitics of lubricating oils
［S］.

服务与反馈：

【文章下载】【加入收藏】