Transactions of Materials and Heat Treatment

Title：Influence of multi-directional forging on thermal fatigue property and high-temperature oxidation resistance for H13 die steel

Authors： Cao Yuan1 Li Qiangjun2

Unit： 1. School of Automotive and Aviation Engineering Henan Polytechnic Institute 2. College of Materials Henan University

KeyWords： multi-directional forging forging pass H13 die steel thermal fatigue property high-temperature oxidation resistance

ClassificationCode：TG316.3

year,vol(issue):pagenumber：2025,50(2):16-23

Abstract：

Multi-directional forging is an effective way to modify metal materials. Therefore, in order to investigate the influence laws of multi-directional forging on the thermal fatigue property and high-temperature oxidation resistance for H13 die steel, the H13 die steel samples were subjected to multi-directional forging by different forging passes, and the thermal fatigue tests were conducted 1000 times with heating at 650 ℃ and cooling at -20 ℃ cycles, as well as the high-temperature oxidation tests were also conducted with insulation at 600 ℃ for 100 hours. Finally, the microstructure inside the samples was analyzed by scanning electron microscopy. The research shows that compared with before multi-directional forging, the multi-directional forging with two passes upgrades the thermal fatigue level of H13 die steel samples from level 9 to level 4, and the mass gain per unit area decreases from 121 mg·mm-2 to 63 mg·mm-2, representing a reduction of 47.93% compared to the state before multi-directional forging. Multi-directional forging refines the carbide size inside H13 die steel specimens, improves the uniformity of carbide distribution, and significantly enhances the thermal fatigue property and high-temperature oxidation resistance of H13 die steel samples. However, the thermal fatigue property and high-temperature oxidation resistance of H13 die steel samples do not continue to significantly improve with the further increasing of multi-directional forging passes.

Funds：

河南省高等教育教学改革研究与实践项目（教高2019740）；国家职业教育新能源汽车技术专业教学资源库（2018-07-KCJS11）

作者简介：曹源（1988-），女，学士，讲师,E-mail：897507193@qq.com

Reference：

[1]窦靖杰,陈广,王均. 盐浴氮化+氧化和QPQ处理对H13模具钢抗铝液腐蚀性能的影响[J]. 热加工工艺,2023,52(6):88-91,97.

Dou J J, Chen G, Wang J. Effects of salt bath nitriding+oxidation and QPQ treatment on corrosion resistance of H13 die steel in aluminum solution[J]. Hot Working Technology,2023,52(6):88-91,97.

[2]陈国鑫,桑宝光,刘明泽,等. Si-Cr-Mo改进型H13热作模具钢热变形行为及有限元模拟[J]. 锻压技术,2023,48(2):215-223.

Chen G X, Sang B G, Liu M Z, et al. Thermal deformation behavior and finite element simulation on Si-Cr-Mo modified H13 hot work die steel[J]. Forging & Stamping Technology,2023,48(2):215-223.

[3]郑立春,彭博,娄健,等. 含铈镁H13模具钢电渣重熔渣系的研究[J]. 东北大学学报（自然科学版）,2023,44(8):1111-1118.

Zheng L C, Peng B, Lou J, et al. Study on the electroslag remelting slag for H13 die steel containing Ce and Mg[J]. Journal of Northeastern University(Natural Science),2023,44(8):1111-1118.

[4]赵帆,周文健,张志豪. 稀土镧对H13模具钢回火稳定性和抗氧化性的影响[J]. 材料导报,2023,37(2):124-129.

Zhao F, Zhou W J, Zhang Z H. Effect of lanthanum on tempering resistance and oxidation resistance of the H13 die steel[J]. Materials Reports,2023,37(2):124-129.

[5]姜高强,崔承云,魏礼桢,等. 激光熔覆Fe基合金涂层强化H13热作模具钢[J]. 材料科学与工艺,2022,30(2):35-42.

Jiang G Q, Cui C Y, Wei L Z, et al. Laser cladding Fe-based alloy coating for strengthening H13 hot work die steel[J]. Materials Science and Technology,2022,30(2):35-42.

[6]杨永强,黄坤,吴世彪,等. H13模具钢粘结剂喷射增材制造工艺参数对成形质量的影响[J]. 航空制造技术,2022,65(23):90-97,109.

Yang Y Q, Huang K, Wu S B, et al. Influence of binder jetting additive manufacturing process parameters on forming quality of H13 mold steel[J]. Aeronautical Manufacturing Technology,2022,65(23):90-97,109.

[7]王洪涛,韩毅华,曹立军,等. H13热作模具钢电渣重熔渣系优化[J]. 钢铁,2022,57(8):111-122.

Wang H T, Han Y H, Cao L J, et al. Optimization of electroslag remelting slag system of H13 hot work die steel[J]. Iron & Steel,2022,57(8):111-122.

[8]吴方俊,邓小云,揭晓华,等. 热作模具用H13和Dievar钢的热疲劳性能[J]. 金属热处理,2022,47(3):165-172.

Wu F J, Deng X Y, Jie X H, et al. Thermal fatigue properties of H13 and Dievar steels for hot-work die[J]. Heat Treatment of Metals,2022,47(3):165-172.

[9]段怡如,李宝宽,黄雪驰,等. 电渣重熔H13模具钢过程碳偏析的模拟研究[J]. 过程工程学报,2022,22(8):1074-1084.

Duan Y R, Li B K, Huang X C, et al. Simulation of carbon segregation during electroslag remelting of H13 die steel[J]. The Chinese Journal of Process Engineering,2022,22(8):1074-1084.

[10]姚南,胡树兵,成永健,等. 激光加工微织构对H13模具钢表面多层涂层性能的影响[J]. 材料热处理学报,2022,43(5):158-169,176.

Yao N, Hu S B, Cheng Y J, et al. Effect of laser fabricated micro texture on properties of multilayer coating on H13 die steel surface[J]. Transactions of Materials and Heat Treatment,2022,43(5):158-169,176.

[11]张杰,徐兵,段佳伟,等. 基于响应面法的H13模具钢激光增材再制造工艺优化[J]. 真空科学与技术学报,2022,42(7):547-554.

Zhang J, Xu B, Duan J W, et al. Optimization of laser additive remanufacturing process parameters of H13 die steel based on response surface method[J]. Chinese Journal of Vacuum Science and Technology,2022,42(7):547-554.

[12]李阔,孙明月,徐斌,等. 稀土H13模具钢横向冲击性能影响因素分析[J]. 金属热处理,2022,47(3):181-185.

Li K, Sun M Y, Xu B, et al. Analysis of influencing factors on transverse impact properties of rare earth H13 die steel[J]. Heat Treatment of Metals,2022,47(3):181-185.

[13]朱振强,宁辉,左鹏鹏,等. 应变幅对H13热作模具钢等温疲劳行为的影响[J]. 工程科学学报,2021,43(5):656-662.

Zhu Z Q, Ning H, Zuo P P, et al. Effect of strain amplitude on the isothermal fatigue behavior of H13 hot work die steel[J]. Chinese Journal of Engineering,2021,43(5):656-662.

[14]曹飞杨,谢敬佩,王淼辉,等. 喷射成形 H13钢的抗氧化性[J]. 金属热处理,2016,41(3):134-137.

Cao F Y, Xie J P, Wang M H, et al. Oxidation resistance of spray-formed H13 steel[J]. Heat Treatment of Metals,2016,41(3):134-137.

[15]GB/T 15824—2008, 热作模具钢热疲劳试验方法[S].

GB/T 15824—2008,Thermal fatigue testing method for hot die steel [S].

[16]徐烽.多向锻造变形对ZK60镁合金组织和性能影响研究[D]. 南京:南京理工大学, 2012.

Xu F. Research on the Effect of Multidirectional Forging Deformation on the Structure and Properties of ZK60 Magnesium Alloy[D]. Nanjing: Nanjing University of Science and Technology, 2012.

[17]朱庆丰,王嘉,左玉波,等. 多向锻造道次对5182铝合金变形组织的影响[J]. 东北大学学报（自然科学版）,2015,36(11):1572-1575,1580.

Zhu Q F, Wang J, Zuo Y B, et al. Effects of forging pass on the structure of 5182 aluminum alloy during multi-direction forging process[J]. Journal of Northeastern University(Natural Science),2015,36(11):1572-1575,1580.

[18]Yousefi D, Taghiabadi R, Shaeri M H. Effect of multi-pass multi-directional forging on tribological properties of Si-rich eutectoid ZA alloys [J]. Transactions of Nonferrous Metals Society of China,2021,31(7):2024-2038.

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